HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 22908992, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 22909004 | HCID 22909004 | — |
| Product | HCID 22908992 | HCID 22908992 | 70% |
Reaction Steps
Substantially the same procedure as in Example 2 was repeated using 1.00 g (1.96 mmol) of Compound 1 obtained in Example 1 and 0.6 ml of conc. aqueous ammonia. The resulting crude crystals were recrystallized from dioxane/water to give 670 mg (yield 70%) of Compound 9 as yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05670498 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-11a5daa9c6d34689bafbd12af22c6c18 |
| Source note | uspto-grants-1997_09 |