HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 22910410, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 2-Fluorobenzenesulphonyl chloride | HCID 137761 | — |
| Reactant | HCID 22910444 | HCID 22910444 | — |
| Reactant | HCID 22910486 | HCID 22910486 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 22910410 | HCID 22910410 | — |
Reaction Steps
Isopropyl 2-fluorobenzenesulfonate was made from 2-fluorobenzenesulfonyl chloride and treated first with butyl lithium and then with iodomethane in a manner analogous to that set forth above in Example to yield isopropyl 2-fluoro-6-methylbenzenesulfonate (formed as a 2:1 mixture with isopropyl 2-fluoro-3-methylbenzenesulfonate as the minor isomer).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05670691 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-41bcc24fbd304cea9ca3aa55c94c5396 |
| Source note | uspto-grants-1997_09 |