2-Bromohexanoic acid → HCID 22910263, compound

HRID 1379392Notes

Reaction equation

[Br:1][CH:2]([CH2:6][CH2:7][CH2:8][CH3:9])[C:3]([OH:5])=O.[CH3:10][N:11]1[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]1>>[Br:1][CH:2]([CH2:6][CH2:7][CH2:8][CH3:9])[C:3]([N:14]1[CH2:15][CH2:16][N:11]([CH3:10])[CH2:12][CH2:13]1)=[O:5]

Participants

Reactant 2

HCID 120132-Bromohexanoic acid

HCID 531671-Methylpiperazine

Product 1

HCID 22910263HCID 22910263, compound

Procedure

Using the mixed anhydride procedure of Example 6F, 2-bromohexanoic acid was coupled to 1-methylpiperazine to provide the desired compound.

Sources & evidence

ORD record: ord-1430f780ff5647ca8a5ecc92fd1fbf93
Source dataset: uspto-grants-1997_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05670675

Reaction notes

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