HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Pyridinyl)-2-propenoic acid → 3-(Pyridin-3-yl)propanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Pyridinyl)-2-propenoic acid | HCID 101984 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 3-(Pyridin-3-yl)propanoic acid | HCID 259624 | — |
Reaction Steps
A mixture of 3 g (20 mmol) of 3-(3-pyridinyl)acrylic acid and 0.3 g of 10% palladium on carbon in 150 ml of ethyl acetate was shaken under 4 atmospheres of hydrogen for 24 h. After filtration, the resulting solution was concentrated in vacuo to provide the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05670675 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-7c03a54e9a2441a88373bad2400446a1 |
| Source note | uspto-grants-1997_09 |