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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1379477Generated: October 29, 2026

Methyl iodide → HCID 22872083, compound

https://huagongshe.com/reaction/1379477

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 53993388HCID 53993388—
ProductHCID 22872083HCID 22872083—

Reaction Steps

A 200 mg portion of (4aR)-(10bR)-10b-methyl-8-(phenylsulfonyl)-1,2,3,4,4a,5,6,10b-octahydrobenzo[f]-quinolin-3-one was methylated with methyl iodide to obtain 144 mg of the desired product. mp 165°-167° FDMS: m/e=369. α[D]589 =+76.2, α[D]365 =+269.7 (chloroform).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05670514
Source datasetuspto-grants-1997_09
ORD IDord-d2c3cfcc06d2451ab9f3fd7ae8c7de60
Source noteuspto-grants-1997_09