HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 10736880, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 10503917 | HCID 10503917 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10736880 | HCID 10736880 | — |
Reaction Steps
The t-Boc group of 1 g (2.2 mmol) of Boc-Asp(OBzl)-OTce is deprotected using 50 ml of 50% TFA in DCM, and the reaction mixture is stirred for 45 minutes. Volatile compounds in the reaction mixture are removed by rotary evaporator under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05672584 |
| Source dataset | uspto-grants-1997_09 |
| ORD ID | ord-20eb8fccca0347ccb033780aa7695145 |
| Source note | uspto-grants-1997_09 |