HRID1379599
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The t-Boc group of 1 g (2.2 mmol) of Boc-Asp(OBzl)-OTce is deprotected using 50 ml of 50% TFA in DCM, and the reaction mixture is stirred for 45 minutes. Volatile compounds in the reaction mixture are removed by rotary evaporator under vacuum.
WORKUP
后处理
- customVolatile compounds in the reaction mixture are removed by rotary evaporator under vacuum