Methyl Isocyanate → HCID 20241044, compound

HRID 1379969Notes

Reaction equation

HRID 1379969 reaction equation
[CH3:1][O:2][CH2:3][C:4]([C:6]1[CH:12]=[CH:11][C:9]([NH2:10])=[CH:8][CH:7]=1)=[CH2:5].C[N:14]=[C:15]=[O:16].[C:17]([O-])(=O)C.C([O-])(=O)C.C([Sn+2]CCCC)CCC>C(OCC)C>[CH3:1][O:2][CH2:3][C:4]([C:6]1[CH:7]=[CH:8][C:9]([N:10]([CH3:17])[C:15]([NH2:14])=[O:16])=[CH:11][CH:12]=1)=[CH2:5]

Participants

5

Reactant 3

HCID 12228Methyl IsocyanateHCID 9798523Di-n-butyl diacetoxy tinHCID 13187348HCID 13187348, compound

Product 1

HCID 20241044HCID 20241044, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

To a solution of 8.2 g (0.05 Mol) 4-(1-methoxymethyl-ethenyl)aniline in 200 ml absolute diethylether are added, at ambient temperature, 4 ml (0.067 Mol) methylisocyanate. The resulting reaction solution is, after the addition of 0.3 g dibutyl tin diacetate, kept at room temperature for 20 hours.

Workup

  1. customThe resulting reaction solution

Sources & evidence

ORD record
ord-e39293b638bc4dcfbf7ddab5c9f2390b
Source dataset
uspto-grants-1986_04
Patent number
US04579585

Reaction notes

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