HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → HCID 20241044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | Di-n-butyl diacetoxy tin | HCID 9798523 | — |
| Reactant | HCID 13187348 | HCID 13187348 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20241044 | HCID 20241044 | — |
Reaction Steps
To a solution of 8.2 g (0.05 Mol) 4-(1-methoxymethyl-ethenyl)aniline in 200 ml absolute diethylether are added, at ambient temperature, 4 ml (0.067 Mol) methylisocyanate. The resulting reaction solution is, after the addition of 0.3 g dibutyl tin diacetate, kept at room temperature for 20 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04579585 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-e39293b638bc4dcfbf7ddab5c9f2390b |
| Source note | uspto-grants-1986_04 |