HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromide ion → HCID 13187365, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromide ion | HCID 259 | — |
| Reactant | Potassium Fluoride | HCID 522689 | — |
| Reactant | HCID 13187346 | HCID 13187346 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13187365 | HCID 13187365 | — |
Reaction Steps
Under a N2 blanket is stirred a mixture of 296.5 g (1.5 Mol) 4(1-chloromethyl-ethenyl)-nitrobenzene, 430 g (7.4 Mol) KF, 78 g (0.15 Mol) hexadecyltributylphosphonimine bromide and 800 ml H2O, during 5 hours at 110°-112°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04579585 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-0de37c3abbb04374a60a8bb586bbd101 |
| Source note | uspto-grants-1986_04 |