HuagongsheHuagongshe Chemistry Print Report · For research reference only
4(Fluoromethyl-ethyl)-nitrobenzene → 4(1-Fluoromethyl-ethyl)-aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4(Fluoromethyl-ethyl)-nitrobenzene | HCID 13187367 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4(1-Fluoromethyl-ethyl)-aniline | HCID 13187368 | — |
Reaction Steps
10.3 g (0.057 Mol) 4(1-fluoromethyl-ethyl)-nitrobenzene are dissolved in 250 ml absolute CH3OH and hydrogenated at room temperature and atmospheric pressure in the presence of 0.61 g 10% Pd/C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04579585 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-7ba063574cf745628233321543db1a15 |
| Source note | uspto-grants-1986_04 |