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HRID1379978

反应详情

EQUATION

反应方程式

HRID 1379978 的结构方程式

REACTANTS

反应物

3
结构：O=S(=O)(O)O
HCID1118

Sulfuric acid

H2O4S

结构：CC(CF)c1ccc([N+](=O)[O-])cc1
HCID13187367

未命名化合物

结构：[K+].[O-][Br+2]([O-])[O-]
HCID23673461

Potassium bromate

BrKO3

PRODUCTS

生成物

1
结构：CC(CF)c1ccc([N+](=O)[O-])cc1Br
HCID13187372

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

To 80 ml of concentrated sulfuric acid, 80 ml of water and 18.3 g (0.1 Mol) of 4(fluoromethyl-ethyl)-nitrobenzene are added portionwise with stirring 18.3 g (0.11 Mol) potassium bromate at such a rate that the temperature does not exceed 35°.

WORKUP

后处理

  1. customdoes not exceed 35°