HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → 3-Bromo-4(1-fluoromethyl-ethyl)-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 4(Fluoromethyl-ethyl)-nitrobenzene | HCID 13187367 | — |
| Reactant | Potassium Bromate | HCID 23673461 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-Bromo-4(1-fluoromethyl-ethyl)-nitrobenzene | HCID 13187372 | — |
Reaction Steps
To 80 ml of concentrated sulfuric acid, 80 ml of water and 18.3 g (0.1 Mol) of 4(fluoromethyl-ethyl)-nitrobenzene are added portionwise with stirring 18.3 g (0.11 Mol) potassium bromate at such a rate that the temperature does not exceed 35°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04579585 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-64aa0aaee55d45b0a4adb5908f873599 |
| Source note | uspto-grants-1986_04 |