HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic acid, 2-oxo-, methyl ester → HCID 23327043, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic acid, 2-oxo-, methyl ester | HCID 70205 | — |
| Reactant | 3-Methoxybenzamide | HCID 98487 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23327043 | HCID 23327043 | — |
Reaction Steps
3-Methoxybenzamide (13.25 g) and methyl glyoxylate (7.72 g) in toluene (150 ml) were heated under reflux in a Dean-Stark apparatus for 6 hours. On cooling the mixture the product separated and was crystallised from toluene. Yield, 12.0 g, m.p. 93°-94°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04579581 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-76c714444ef64230a1065be1a2126181 |
| Source note | uspto-grants-1986_04 |