HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Pyrrolidino-1-cyclohexene → Diethyl 1-pyrrolidinocyclohexane-1-phosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Pyrrolidino-1-cyclohexene | HCID 70768 | — |
| Reactant | Diethylphosphite | HCID 3780918 | — |
| Product | Diethyl 1-pyrrolidinocyclohexane-1-phosphonate | HCID 13685032 | — |
Reaction Steps
A mixture of 1-pyrrolidinocyclohexene (15.1 g; 0.1 mole) and diethyl phosphite (13.8 g; 0.1 mole) was heated for 2 hours on a steam bath. The resulting liquid showed no absorption in the infrared for C=C or P-H. Distillation yielded pure diethyl 1-pyrrolidinocyclohexane-1-phosphonate, bp 80°-85°/0.1 mm. ##STR8##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04579956 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-d70652e9476e4f98af7727b59e70eb4f |
| Source note | uspto-grants-1986_04 |