2-Propenoic acid, 3-phenyl-, methyl ester → HCID 13335371, compound

HRID 1380156Notes

Reaction equation

HRID 1380156 reaction equation
[Cl:1][GeH:2]([Cl:4])[Cl:3].[C:5]([O:15][CH3:16])(=[O:14])[CH:6]=[CH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1>>[Cl:1][Ge:2]([Cl:4])([Cl:3])[CH:7]([C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[CH2:6][C:5]([O:15][CH3:16])=[O:14]

Participants

3

Reactant 2

HCID 76442-Propenoic acid, 3-phenyl-, methyl esterHCID 70900CID 70900

Product 1

HCID 13335371HCID 13335371, compoundYield 82.2%

Procedure

A mixture of 36.0 g (0.2 mol) of trichlorogermane and 32.4 g (0.2 mol) of methyl cinnamate was stirred for 2 hours and then distilled in vacuum to obtain 56.2 g of a fraction, b.p. 148°. Yield 82.2%.

Workup

  1. distillationdistilled in vacuum
  2. customto obtain 56.2 g of a fraction, b.p. 148°

Sources & evidence

ORD record
ord-5dfe41e9163e4322a1ec6ac951256446
Source dataset
uspto-grants-1986_04
Patent number
US04579961

Reaction notes

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