HCID 3335773, compound → 2,3,5,6-Tetraaminocyclohexa-2,5-diene-1,4-dione
Reaction equation
C1(=O)[N:5]([C:6]2[C:11](=[O:12])[C:10]([N:13]3C(=O)C4=CC=CC=C4C3=O)=[C:9]([N:24]3C(=O)C4=CC=CC=C4C3=O)[C:8](=[O:35])[C:7]=2[N:36]2C(=O)C3=CC=CC=C3C2=O)C(=O)C2=CC=CC=C12>O.NN>[NH2:36][C:7]1[C:8](=[O:35])[C:9]([NH2:24])=[C:10]([NH2:13])[C:11](=[O:12])[C:6]=1[NH2:5]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 60 °C
Procedure
Tetraphthalimido-1,4-benzoquinone (30.00 g, 0.044 mole) is added to 200 ml of 80% hydrazine hydrate. The mixture is heated to 60° C. for two hours. After cooling to room temperature, the mixture is filtered yielding dark purple crystals melting at 260°-262° C.
Workup
- temperatureAfter cooling to room temperature
- filtrationthe mixture is filtered
Sources & evidence
- ORD record
- ord-79c4bc85ea474ea58c0d970f0468d8de
- Source dataset
- uspto-grants-1986_04
- Patent number
- US04581349
Reaction notes
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