Dimethylformamide → HCID 6994923, compound

HRID 1380454Notes

Reaction equation

HRID 1380454 reaction equation
[NH:1]([C:10]([O:12][CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[O:11])[C@H:2]([C:7]([OH:9])=O)[CH2:3][CH:4]([CH3:6])[CH3:5].CN([CH:23]=[O:24])C>>[NH:1]([C:10]([O:12][CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)=[O:11])[C@H:2]([C:7]([NH:1][CH2:2][C:7]([O:24][CH3:23])=[O:9])=[O:9])[CH2:3][CH:4]([CH3:5])[CH3:6]

Participants

3

Reactant 2

HCID 6228DimethylformamideHCID 74840Leucine, N-carboxy-, N-benzyl ester, L-

Product 1

HCID 6994923HCID 6994923, compound

Procedure

0.22 mole of Z-Leu-OH are dissolved in 500 ml of DMF. To this solution are successively added:

Workup

  1. additionTo this solution are successively added

Sources & evidence

ORD record
ord-52d83d7610a24b61979375cb54a05f7d
Source dataset
uspto-grants-1986_04
Patent number
US04581168

Reaction notes

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