Ethanolamine → HCID 21281528, compound

Participants

Reaction Steps

42.8 g of ethanolamine are placed in 350 ml of methylene chloride. 47.8 g of isobutyl chloroformate are then added dropwise during 1 hour at 5°-15° C. while cooling with ice. After stirring at room temperature for a further 4 hours, the methylene chloride is removed by evaporation and the residue is distilled. There is obtained pure isobutyl 2-hydroxyethylcarbamate; b.p. 111°-113° C./0.07 Torr.

Provenance & Evidence