Ethanol → HCID 23325158, compound

Participants

Reaction Steps

0.8 g of Raney-nickel are placed in a hydrogenation flask and suspended in 50 ml of ethanol. 7.6 g of 4'-chloro-2,2'-diethoxy-2'-nitroacetanilide are added thereto and the mixture is hydrogenated at room temperature and normal pressure. The uptake of hydrogen has finished after 2 hours. After suction filtration and concentration of the filtrate, the product is precipitated with water. There is obtained 4'-chloro-2,2-diethoxy-2'-aminoacetanilide of melting point 89°-90° C.

Provenance & Evidence