HCID 23325188, compound → 103451-26-9

Participants

Reaction Steps

A solution of 0.4 g of 1 in 2 ml of concentrated hydrochloric acid was stirred at room temperature for one hour. The water was evaporated. Toluene was added to the residue and distilled to remove residual water by azeotropic distillation. The residue was dried under reduced pressure to give 2, as a hygroscopic solid.

Provenance & Evidence