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HRID1380597

反应详情

EQUATION

反应方程式

HRID 1380597 的结构方程式

REACTANTS

反应物

2
结构：C1COCCN1
HCID8083

Morpholine

C4H9NO

结构：COC1(c2ccc(SC)cc2)OC1(C)C
HCID20192525

2-Methoxy-3,3-dimethyl-2-[4-(methylsulfanyl)phenyl]oxirane

C12H16O2S

PRODUCTS

生成物

1
结构：CSc1ccc(C(=O)C(C)(C)N2CCOCC2)cc1
HCID92387

2-Methyl-4'-(methylthio)-2-morpholinopropiophenone

C15H21NO2S

PROCEDURE

实验过程

151.4 g (0.675 mol) of 3,3-dimethyl-2-methoxy-2-[4-(methylthio)-phenyl]-oxirane (melting point 62°-64° C.) are dissolved in 235.2 g (2.70 mols) of morpholine and the solution is warmed to reflux temperature.

WORKUP

后处理

  1. temperaturethe solution is warmed
  2. temperatureto reflux temperature