HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-Propanone, 2-chloro-1-(4-chlorophenyl)-2-methyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Reactant | 1-(4-Chlorophenyl)-2-methylpropan-1-one | HCID 72865 | — |
| Product | 1-Propanone, 2-chloro-1-(4-chlorophenyl)-2-methyl- | HCID 587356 | — |
Reaction Steps
182.7 g (1.0 mol) of 1-(4-chlorophenyl)-2-methylpropan-1-one are warmed to 40° and chlorinated with 71 g (1.0 mol) of chlorine gas at 40°-65° in the course of 5 hours. The dissolved HCl gas is then driven off by blowing with nitrogen. The liquid crude product is then reacted further.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04582862 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-c62e586cd23d46bda40e053b9ce6c82f |
| Source note | uspto-grants-1986_04 |