Hydrochloric Acid → 1-Propanone, 2-chloro-1-(4-chlorophenyl)-2-methyl-

HRID 1380598Notes

Reaction equation

HRID 1380598 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8](=[O:12])[CH:9]([CH3:11])[CH3:10])=[CH:4][CH:3]=1.[Cl:13]Cl.Cl>>[Cl:13][C:9]([CH3:10])([CH3:11])[C:8]([C:5]1[CH:4]=[CH:3][C:2]([Cl:1])=[CH:7][CH:6]=1)=[O:12]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 24526ChlorineHCID 728651-(4-Chlorophenyl)-2-methylpropan-1-one

Product 1

HCID 5873561-Propanone, 2-chloro-1-(4-chlorophenyl)-2-methyl-

Procedure

182.7 g (1.0 mol) of 1-(4-chlorophenyl)-2-methylpropan-1-one are warmed to 40° and chlorinated with 71 g (1.0 mol) of chlorine gas at 40°-65° in the course of 5 hours. The dissolved HCl gas is then driven off by blowing with nitrogen. The liquid crude product is then reacted further.

Workup

  1. customThe liquid crude product is then reacted further

Sources & evidence

ORD record
ord-c62e586cd23d46bda40e053b9ce6c82f
Source dataset
uspto-grants-1986_04
Patent number
US04582862

Reaction notes

Loading…