N,N-Dimethylethylenediamine → HCID 13590121, compound

HRID 1380617Notes

Reaction equation

HRID 1380617 reaction equation
Cl[C:2]1[C:15]2[C:14](=[O:16])[C:13]3[C:8](=[CH:9][CH:10]=[C:11]([OH:17])[CH:12]=3)[S:7][C:6]=2[C:5]([N+:18]([O-:20])=[O:19])=[CH:4][CH:3]=1.[CH3:21][N:22]([CH3:26])[CH2:23][CH2:24][NH2:25]>>[CH3:21][N:22]([CH3:26])[CH2:23][CH2:24][NH:25][C:2]1[C:15]2[C:14](=[O:16])[C:13]3[C:8](=[CH:9][CH:10]=[C:11]([OH:17])[CH:12]=3)[S:7][C:6]=2[C:5]([N+:18]([O-:20])=[O:19])=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 66053N,N-DimethylethylenediamineHCID 135901181-Chloro-7-hydroxy-4-nitro-9H-thioxanthen-9-one

Product 1

HCID 13590121HCID 13590121, compound

Procedure

1-[[2-(Dimethylamino)ethyl]amino]-7-hydroxy-4-nitro-9H-thioxanthen-9-one was prepared similarly from 10 g of 1-chloro-7-hydroxy-4-nitrothioxanthone and 5.7 g of N,N-dimethylethylenediamine to provide 7.2 g, mp>300°.

Workup

  1. customto provide 7.2 g, mp>300°

Sources & evidence

ORD record
ord-954b4cf3d0b7416e98a2a7f30bbac196
Source dataset
uspto-grants-1986_04
Patent number
US04582851

Reaction notes

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