HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylic Acid → N-(3-(Dimethylamino)-2,2-dimethylpropyl)acrylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | N,N,2,2-Tetramethylpropane-1,3-diamine | HCID 104477 | — |
| Solvent | Boron trifluoride | HCID 6356 | — |
| Product | N-(3-(Dimethylamino)-2,2-dimethylpropyl)acrylamide | HCID 88388 | 72% |
Reaction Steps
Proceeding as in Example 1, 260 g 3-dimethylamino-2,2-dimethylpropylamine; 144 g acrylic acid; 4 g N,N'-diphenylenediamine; and 10 ml BF3-etherate were mixed. It was found possible to isolate 265 g (72%) of the N-(3-dimethylamino-2,2-dimethylpropyl)acrylamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04582933 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-dc934397b71e4fc6b0ef80d07587b4e8 |
| Source note | uspto-grants-1986_04 |