Phosphoric Acid → HCID 23325893, compound

HRID 1380700Notes

Reaction equation

HRID 1380700 reaction equation
[CH2:1]([N:3]([CH2:10][CH3:11])[CH2:4][C:5]([CH3:9])([CH3:8])[CH2:6][NH2:7])[CH3:2].[C:12](O)(=[O:15])[CH:13]=[CH2:14].P(=O)(O)(O)O>C1C=CC(NC2C=CC(NC3C=CC=CC=3)=CC=2)=CC=1>[CH2:10]([N:3]([CH2:1][CH3:2])[CH2:4][C:5]([CH3:9])([CH3:8])[CH2:6][NH:7][C:12](=[O:15])[CH:13]=[CH2:14])[CH3:11]

Participants

5

Reactant 3

HCID 1004Phosphoric AcidHCID 6581Acrylic AcidHCID 23325891HCID 23325891, compound

Product 1

HCID 23325893HCID 23325893, compoundYield 59.1%

Reagents, catalysts & solvents 1

HCID 6319N,N'-Diphenyl-P-PhenylenediamineCatalyst

Procedure

Proceeding as in Example 1, 60 g 3-diethylamino-2,2-dimethylpropylamine; 27.3 g acrylic acid; 1.0 g N,N'-diphenyl-p-phenylenediamine; and 1 ml 85% phosphoric acid were mixed. 47.5 g (59%) N-(3-diethylamino-2,2-dimethylpropyl)acrylamide, boiling point 139° to 141° C. at 1.33 Pa, were isolated.

Sources & evidence

ORD record
ord-620832a89685484abc013d9a166fc232
Source dataset
uspto-grants-1986_04
Patent number
US04582933

Reaction notes

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