Acrylic Acid → HCID 23325890, compound

HRID 1380701Notes

Reaction equation

HRID 1380701 reaction equation
[CH3:1][N:2]([CH3:13])[CH2:3][C:4]([CH2:11][CH3:12])([CH2:7][CH2:8][CH2:9][CH3:10])[CH2:5][NH2:6].[C:14](O)(=[O:17])[CH:15]=[CH2:16]>C1C=CC(NC2C=CC(NC3C=CC=CC=3)=CC=2)=CC=1>[CH3:13][N:2]([CH3:1])[CH2:3][C:4]([CH2:11][CH3:12])([CH2:7][CH2:8][CH2:9][CH3:10])[CH2:5][NH:6][C:14](=[O:17])[CH:15]=[CH2:16]

Participants

4

Reactant 2

HCID 6581Acrylic AcidHCID 23325892HCID 23325892, compound

Product 1

HCID 23325890HCID 23325890, compoundYield 55%

Reagents, catalysts & solvents 1

HCID 6319N,N'-Diphenyl-P-PhenylenediamineCatalyst

Procedure

Proceeding as in Example 1, 173.5 g 3-dimethylamino-2-ethyl-2-butylpropylamine; 67 g acrylic acid; 2 g N,N'-diphenyl-p-phenylenediamine; and 2 g calcium tert-butylate were mixed. 122 g (55%) N-(3-dimethylamino-2-ethyl-2-butylpropyl)-acrylamide, boiling point 129° C. at 66.5 Pa, was isolated.

Sources & evidence

ORD record
ord-5797400c5c7f491196235ec1ec87e301
Source dataset
uspto-grants-1986_04
Patent number
US04582933

Reaction notes

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