HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 3-methoxy-4-(7H-purin-8-yl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 3-Methoxy-4-(7H-purin-8-yl)benzamide | HCID 13284531 | — |
| Product | Ethyl 3-methoxy-4-(7H-purin-8-yl)benzoate | HCID 13284533 | — |
Reaction Steps
A quantity of 0.42 gm of 8-(2'-methoxy-4'-chlorocarbonyl-phenyl)-purine hydrochloride (see Example 43) was refluxed in 30 ml of ethanol for 45 minutes. The solvent was evaporated off, and the residue was purified over a silica gel column [eluant: methylene chloride/ethanol (50:1 to 19:1)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04582837 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-441c04dd5d6a457d8d41d361bc4b29a7 |
| Source note | uspto-grants-1986_04 |