HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetyl chloride → HCID 88688691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetyl chloride | HCID 7679 | — |
| Reactant | HCID 54290755 | HCID 54290755 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 88688691 | HCID 88688691 | — |
Reaction Steps
By a procedure analogous to that used in the second part of Example IV, (S)-[1-[[[bis-(dimethylamino)phophinyl]amino]carbonyl]2-oxo-3-azetidinyl]carbamic acid phenylmethyl ester, produced as in the previous Example, is hydrogenated in the presence of 10% Pd on carbon catalyst, and the intermediate thus obtained is acylated by reaction with phenylacetyl chloride and triethylamine to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04584132 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-a0b6cfeb6dc047f6a5bce5065a9d4a37 |
| Source note | uspto-grants-1986_04 |