Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1380806Generated: November 2, 2026

Phenylacetyl chloride → HCID 88688691, compound

https://huagongshe.com/reaction/1380806

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenylacetyl chlorideHCID 7679—
ReactantHCID 54290755HCID 54290755—
CatalystPalladiumHCID 23938—
SolventTriethylamineHCID 8471—
ProductHCID 88688691HCID 88688691—

Reaction Steps

By a procedure analogous to that used in the second part of Example IV, (S)-[1-[[[bis-(dimethylamino)phophinyl]amino]carbonyl]2-oxo-3-azetidinyl]carbamic acid phenylmethyl ester, produced as in the previous Example, is hydrogenated in the presence of 10% Pd on carbon catalyst, and the intermediate thus obtained is acylated by reaction with phenylacetyl chloride and triethylamine to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04584132
Source datasetuspto-grants-1986_04
ORD IDord-a0b6cfeb6dc047f6a5bce5065a9d4a37
Source noteuspto-grants-1986_04