Dimethylthiocarbamoyl chloride → HCID 53894584, compound

HRID 1380836Notes

Reaction equation

[Cl:1][CH2:2][C:3]1[CH:8]=[C:7]([OH:9])[N:6]=[C:5]([CH3:10])[N:4]=1.[CH3:11][N:12]([CH3:16])[C:13](Cl)=[S:14]>>[CH3:11][N:12]([CH3:16])[C:13](=[S:14])[O:9][C:7]1[N:6]=[C:5]([CH3:10])[N:4]=[C:3]([CH2:2][Cl:1])[CH:8]=1

Participants

Reactant 2

HCID 27871Dimethylthiocarbamoyl chloride

HCID 178433451HCID 178433451, compound

Product 1

HCID 53894584HCID 53894584, compound

Procedure

4-Chloromethyl-6-hydroxy-2-methyl-pyrimidine is reacted with N,N-dimethylthiocarbamoyl chloride analogously to the process described in Example 86 in order to produce 4-chloromethyl-2-methyl-6-pyrimidinyl N,N-dimethylthiocarbamate which is required as the starting material in Example 30. This product is obtained in the form of a yellow oil.

Sources & evidence

ORD record: ord-4da97e024df44118840f5afe7034730c
Source dataset: uspto-grants-1986_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04584295

Reaction notes

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