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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1380882Generated: October 27, 2026

2-Benzylamino-6,7-dimethoxy-1,2,3,4-tetrahydronaphthalene → 1-[7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-benzyl-N-(6,7-dimethoxy-1,2,3,4-tetrahydronaphth-2-yl)-amino]-propane

https://huagongshe.com/reaction/1380882

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Benzylamino-6,7-dimethoxy-1,2,3,4-tetrahydronaphthaleneHCID 12441978—
Reactant3-(3-Chloropropyl)-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-oneHCID 13092510—
SolventDichloromethaneHCID 6344—
Product1-[7,8-Dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl]-3-[N-benzyl-N-(6,7-dimethoxy-1,2,3,4-tetrahydronaphth-2-yl)-amino]-propaneHCID 13579650—

Reaction Steps

The title compound is prepared analogously to Example 1 by reacting 2-benzylamino-6,7-dimethoxy-1,2,3,4-tetrahydronaphthalene with 1-(7,8-dimethoxy-1,3,4,5-tetra hydro-2H-3-benzazepin-2-on-3-yl)-3-chloropropane. IR spectrum (methylene chloride): 1645 cm-1 (C=O).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04584293
Source datasetuspto-grants-1986_04
ORD IDord-8cdfe36a18fb474f997856eb5335c954
Source noteuspto-grants-1986_04