HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 13579656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-(3-Chloropropyl)-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-one | HCID 13092510 | — |
| Reactant | HCID 23324604 | HCID 23324604 | — |
| Product | HCID 13579656 | HCID 13579656 | — |
Reaction Steps
The title compound is prepared analogously to Example 1 by reacting 1-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-3-chloropropane, triethylamine and 5,6-dimethoxy-2-methyl-amino-1,2,3,4-tetrahydronaphthalene. Mp: 216°-217° C. (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04584293 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-4b794034011d474f9bf939914cd44b6c |
| Source note | uspto-grants-1986_04 |