Triethylamine → HCID 13579656, compound

HRID 1380889Notes

Reaction equation

HRID 1380889 reaction equation
[CH3:1][O:2][C:3]1[C:18]([O:19][CH3:20])=[CH:17][C:6]2[CH2:7][C:8](=[O:16])[N:9]([CH2:12][CH2:13][CH2:14]Cl)[CH2:10][CH2:11][C:5]=2[CH:4]=1.[CH3:21][O:22][C:23]1[C:32]([O:33][CH3:34])=[CH:31][CH:30]=[C:29]2[C:24]=1[CH2:25][CH2:26][CH:27](C)[CH:28]2N.[CH2:37]([N:39](CC)CC)C>>[CH3:1][O:2][C:3]1[C:18]([O:19][CH3:20])=[CH:17][C:6]2[CH2:7][C:8](=[O:16])[N:9]([CH2:12][CH2:13][CH2:14][N:39]([CH3:37])[CH:27]3[CH2:26][CH2:25][C:24]4[C:29](=[CH:30][CH:31]=[C:32]([O:33][CH3:34])[C:23]=4[O:22][CH3:21])[CH2:28]3)[CH2:10][CH2:11][C:5]=2[CH:4]=1

Participants

4

Reactant 3

HCID 8471TriethylamineHCID 130925103-(3-Chloropropyl)-7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-oneHCID 23324604HCID 23324604, compound

Product 1

HCID 13579656HCID 13579656, compound

Procedure

The title compound is prepared analogously to Example 1 by reacting 1-(7,8-dimethoxy-1,3,4,5-tetrahydro-2H-3-benzazepin-2-on-3-yl)-3-chloropropane, triethylamine and 5,6-dimethoxy-2-methyl-amino-1,2,3,4-tetrahydronaphthalene. Mp: 216°-217° C. (decomp.).

Sources & evidence

ORD record
ord-4b794034011d474f9bf939914cd44b6c
Source dataset
uspto-grants-1986_04
Patent number
US04584293

Reaction notes

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