HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13579648, compound → 1-[7,8-Dimethoxy-1,3-dihydro-2H-3-benzazepin-3-yl]-3-[N-methyl-N-(6,7-dimethoxy-1,2,3,4-tetrahydronaphth-2-yl)-amino]-propane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13579648 | HCID 13579648 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | 1-[7,8-Dimethoxy-1,3-dihydro-2H-3-benzazepin-3-yl]-3-[N-methyl-N-(6,7-dimethoxy-1,2,3,4-tetrahydronaphth-2-yl)-amino]-propane | HCID 23324579 | — |
Reaction Steps
The title compound is prepared from 1-[7,8-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(6,7-dimethoxy-1,2,3,4-tetrahydronaphth-2-yl)-amino]-propane and lithium aluminum hydride analogously to Example 13. Mp: 115°-116° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04584293 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-e5912dcead3744118186183f02c17021 |
| Source note | uspto-grants-1986_04 |