Butylamine → HCID 135767527, compound

HRID 1380963Notes

Reaction equation

HRID 1380963 reaction equation
[CH2:1]([NH2:5])[CH2:2][CH2:3][CH3:4].[OH:6][C:7]1[CH:14]=[CH:13][C:12]([CH:15]=[CH2:16])=[CH:11][C:8]=1[CH:9]=O>C1(C)C=CC=CC=1>[CH2:1]([N:5]=[CH:9][C:8]1[CH:11]=[C:12]([CH:15]=[CH2:16])[CH:13]=[CH:14][C:7]=1[OH:6])[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 8007ButylamineHCID 200435625-Ethenyl-2-hydroxybenzaldehyde

Product 1

HCID 135767527HCID 135767527, compoundYield 79%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

74 g (1 mole) of butylamine were added to a solution of 74 g (0.5 mole) of 2-hydroxy-5-vinylbenzaldehyde in 750 ml of toluene, and this mixture was refluxed for 2 hours. It was then extracted with twice 500 ml of ice water and the toluene was distilled off. 80 g (79%) of 2-butyliminomethyl-4-vinylphenol were obtained as a yellow oil.

Workup

  1. temperaturethis mixture was refluxed for 2 hours
  2. extractionIt was then extracted with twice 500 ml of ice water
  3. distillationthe toluene was distilled off

Sources & evidence

ORD record
ord-c71be002104d43ada6ec806a14c6e2b9
Source dataset
uspto-grants-1986_04
Patent number
US04584359

Reaction notes

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