HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butylamine → HCID 135767527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butylamine | HCID 8007 | — |
| Reactant | 5-Ethenyl-2-hydroxybenzaldehyde | HCID 20043562 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 135767527 | HCID 135767527 | 79% |
Reaction Steps
74 g (1 mole) of butylamine were added to a solution of 74 g (0.5 mole) of 2-hydroxy-5-vinylbenzaldehyde in 750 ml of toluene, and this mixture was refluxed for 2 hours. It was then extracted with twice 500 ml of ice water and the toluene was distilled off. 80 g (79%) of 2-butyliminomethyl-4-vinylphenol were obtained as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04584359 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-c71be002104d43ada6ec806a14c6e2b9 |
| Source note | uspto-grants-1986_04 |