Benzoic Acid → HCID 131714642, compound

Participants

Reaction Steps

705 g (5 moles) of vinylmethyldichlorosilane and 1000 ml of hexane are placed in the apparatus of Example 1. The reaction with 1245 g of benzoic acid (=10.2 moles) is performed as described under Example 1; the distillation of the raw product is performed in the same manner. At a pressure of 0.5 mbar and a head temperature of 141° C., 1295 g (4.15 moles) of a colorless liquid is distilled off. The yield amounts to 83%.

Provenance & Evidence