HRID1381086

反应详情

EQUATION

反应方程式

HRID 1381086 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

30 g of the 1-formyl-2-(4-nitrophenyl)hydrazine was then catalytically reduced in 1.6 liters of ethanol in the presence of palladium-on-carbon as a catalyst at room temperature. The reaction mixture was filtered, and the filtrate was evaporated to dryness to obtain 20.5 g of 1-formyl-2-(4-aminophenyl)hydrazine as a white solid. Melting Point: 123°-125° C.

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered
  2. customthe filtrate was evaporated to dryness