HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazinecarboxaldehyde, 2-(4-nitrophenyl)- → Hydrazinecarboxaldehyde, 2-(4-aminophenyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazinecarboxaldehyde, 2-(4-nitrophenyl)- | HCID 5008489 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Hydrazinecarboxaldehyde, 2-(4-aminophenyl)- | HCID 113189 | 81.9% |
Reaction Steps
30 g of the 1-formyl-2-(4-nitrophenyl)hydrazine was then catalytically reduced in 1.6 liters of ethanol in the presence of palladium-on-carbon as a catalyst at room temperature. The reaction mixture was filtered, and the filtrate was evaporated to dryness to obtain 20.5 g of 1-formyl-2-(4-aminophenyl)hydrazine as a white solid. Melting Point: 123°-125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04585731 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-752a2e995f784f8992a77e00b5a79c30 |
| Source note | uspto-grants-1986_04 |