HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(2-Nitrophenyl)-2-pyridinemethanamine → HCID 23323574, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(2-Nitrophenyl)-2-pyridinemethanamine | HCID 13423753 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23323574 | HCID 23323574 | — |
Reaction Steps
10 g of N-2-picolyl-o-nitroaniline are hydrogenated with Raney nickel in methanol at room temperature to give the o-phenylenediamine derivative which remains as an oil, after the catalyst has been filtered off and the solvent has been evaporated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04585775 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-e8df4429a74b4b418a7a793fca64d43d |
| Source note | uspto-grants-1986_04 |