Ethanol → HCID 10398748, compound

HRID 1381105Notes

Reaction equation

HRID 1381105 reaction equation
[C:1]1([NH2:8])[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1N.[NH2:9][C:10]([NH2:12])=[O:11].[CH2:13](O)[CH3:14]>>[N:8]1[CH:1]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:2][N:9]1[C:6]2[CH:1]=[CH:2][CH:3]=[CH:13][C:14]=2[NH:12][C:10]1=[O:11]

Participants

4

Reactant 3

HCID 702EthanolHCID 1176UreaHCID 7243O-Phenylenediamine

Product 1

HCID 10398748HCID 10398748, compound

Procedure

5 g of the above o-phenylenediamine derivative are heated with 2 g of urea to 160° C. for 5 hours. After the reaction mixture has cooled, ethanol is added and the crystals which are precipitated are filtered off with suction.

Workup

  1. temperatureAfter the reaction mixture has cooled
  2. customthe crystals which are precipitated
  3. filtrationare filtered off with suction

Sources & evidence

ORD record
ord-9e5bed632650460988fbe866d0f30f53
Source dataset
uspto-grants-1986_04
Patent number
US04585775

Reaction notes

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