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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1381115Generated: November 3, 2026

Benzyl Bromide → HCID 13035738, compound

https://huagongshe.com/reaction/1381115

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl BromideHCID 7498—
ReactantSodium HydroxideHCID 14798—
ReactantHCID 178517283HCID 178517283—
CatalystTetrabutylammonium BromideHCID 74236—
SolventDichloromethaneHCID 6344—
ProductHCID 13035738HCID 13035738—

Reaction Steps

11.5 g (0.05 mol) of 9-nitro-5-oxo-2,3,5,6-tetrahydroimidazo-[1,2-c]-quinazoline and 6.4 g (0.02 mol) of tetra-n-butylammonium bromide were suspended in 250 ml of 10% strength sodium hydroxide solution. 17.815 g (0.15 mol) of benzyl bromide in 150 ml of methylene chloride were added to the mixture, and the latter was stirred for 2 hours at room temperature.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04585772
Source datasetuspto-grants-1986_04
ORD IDord-c82b8b909f254f6f876a0592bff80882
Source noteuspto-grants-1986_04