HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 13035738, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178517283 | HCID 178517283 | — |
| Catalyst | Tetrabutylammonium Bromide | HCID 74236 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 13035738 | HCID 13035738 | — |
Reaction Steps
11.5 g (0.05 mol) of 9-nitro-5-oxo-2,3,5,6-tetrahydroimidazo-[1,2-c]-quinazoline and 6.4 g (0.02 mol) of tetra-n-butylammonium bromide were suspended in 250 ml of 10% strength sodium hydroxide solution. 17.815 g (0.15 mol) of benzyl bromide in 150 ml of methylene chloride were added to the mixture, and the latter was stirred for 2 hours at room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04585772 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-c82b8b909f254f6f876a0592bff80882 |
| Source note | uspto-grants-1986_04 |