HuagongsheHuagongshe Chemistry Print Report · For research reference only
Monobenzone → HCID 13320250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Monobenzone | HCID 7638 | — |
| Reactant | 3-Benzyl-6-oxa-3-azabicyclo(3.1.0)hexane | HCID 9815370 | — |
| Product | HCID 13320250 | HCID 13320250 | — |
Reaction Steps
A mixture of 40 g. of 1-benzyl-3,4-epoxypyrrolidine and 42 g. of 4-benzoxyphenol was heated at 130° C. for 8 hr. On cooling, the mixture crystallized. Three crystallizations from petroleum ether-cyclohexane gave fluffy white crystals melting at 98.0°-100.0° C. The yield was 6.0 g (8%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04585785 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-7507ad96918c46bfa217b7c66e3653e6 |
| Source note | uspto-grants-1986_04 |