HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 12330040, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | Methyl (11-oxo-6,11-dihydrodibenzo[b,e]oxepin-2-yl)acetate | HCID 10333952 | — |
| Product | HCID 12330040 | HCID 12330040 | — |
Reaction Steps
A mixture of 5.64 g. of methyl 6,11-dihydro-11-oxodibenz[b,e]oxepin-2-acetate, 0.4 g. of sodium borohydride and 250 ml. of methanol is stirred at 0°-2° for four hours. The reaction product is treated with 1 N hydrochloric acid and extracted with chloroform, and the chloroform extracts are washed with saturated sodium bicarbonate solution and dried with sodium sulfate. The chloroform is evaporated to leave methyl 6, 11-dihydro-11-methoxydibenz[b,e]oxepin-2-acetate as an oil;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04585788 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-baf9bfc5120c474fa0433c1a4af697f4 |
| Source note | uspto-grants-1986_04 |