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HRID1381265

反应详情

EQUATION

反应方程式

HRID 1381265 的结构方程式

REACTANTS

反应物

2
结构：NS(=O)(=O)c1ccc(C=O)cc1
HCID151088

4-Sulfamoylbenzaldehyde

C7H7NO3S

结构：CCOP(=O)(CC#N)OCC.[H-].[Na+]
HCID86740749

未命名化合物

PRODUCTS

生成物

1
结构：N#CCCc1ccc(S(N)(=O)=O)cc1
HCID19809182

4-(2-Cyanoethyl)benzene-1-sulfonamide

C9H10N2O2S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

p-Aminosulphonylbenzaldehyde was reacted with diethyl cyanomethyl-phosphonate/sodium hydride in tetrahydrofuran to give 1-cyano-2-(4-aminosulphonylphenyl)-ethane which was hydrogenated in methanol with Raney-cobalt as the catalyst to give 4-(3-aminopropyl)benzenesulphonamide.