HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 1-(3-Diethylaminopropyl)-3-(3-diethylaminopropylamino)indazole dihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 1-(3-Diethylaminopropyl)-3-(3-diethylaminopropylamino)indazole | HCID 3030837 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(3-Diethylaminopropyl)-3-(3-diethylaminopropylamino)indazole dihydrochloride | HCID 23324062 | — |
Reaction Steps
In 50 ml of absolute ethyl alcohol was dissolved 3.0 g of 1-(3-diethylaminopropyl)-3-(3-diethylaminopropylamino)indazole and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Anhydrous diethyl ether was added to the solution to separate crystals. Then the crystals were obtained by filtration and dried to give 1-(3-diethylaminopropyl)-3-(3-diethylaminopropylamino)indazole dihydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04585869 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-b0e8d20b743f4702b81cc05b46a44456 |
| Source note | uspto-grants-1986_04 |