HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 13893921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | WF 3681 | HCID 128356 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 13893921 | HCID 13893921 | — |
Reaction Steps
3-(4-Hydroxy-5-oxo-3-phenyl-2,5-dihydro-2-furyl)-propionic acid (100 mg) was dissolved in pyridine (2 ml), and acetic anhydride (1 ml) was added. The mixture was allowed to stand overnight. The excess reagent and solvent were removed by distillation under reduced pressure, and the residue was dried to give 3-(4-acetoxy-5-oxo-3-phenyl-2,5-dihydro-2-furyl)propionic acid (116 mg) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04585789 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-5b7d2907bcc04a978f8b91fd38a09b55 |
| Source note | uspto-grants-1986_04 |