HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 13893920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | WF 3681 | HCID 128356 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13893920 | HCID 13893920 | — |
Reaction Steps
3-(4-Hydroxy-5-oxo-3-phenyl-2,5-dihydro-2-furyl)propionic acid (100 mg) was dissolved in methanol (2 ml), and a solution of diazomethane in ether was added thereto until the yellow color did not vanish any longer. The mixture was allowed to stand at room temperature overnight. The solvent was then distilled off to give methyl 3-(4-methoxy-5-oxo-3-phenyl-2,5-dihydro-2-furyl)propionate (110 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04585789 |
| Source dataset | uspto-grants-1986_04 |
| ORD ID | ord-ed98f40003de4e4986362a7921d187cc |
| Source note | uspto-grants-1986_04 |