HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178492221, compound → HCID 14838481, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178492221 | HCID 178492221 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14838481 | HCID 14838481 | — |
Reaction Steps
To a stirred solution of the product of step (a) (13.3 g) in dichloromethane (250 ml) was added active manganese dioxide in portions until all traces of starting material had disappeared. The reaction mix was filtered, evaporated to a gum and purified by chromatography on silica, eluting with ether, to give the product, mp 68°-71°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04803216 |
| Source dataset | uspto-grants-1989_02 |
| ORD ID | ord-9676eb3bb7fd4448b220293bfb8a8515 |
| Source note | uspto-grants-1989_02 |